PittsburghV1, France, Analysis, bibRecord, 000581

Efficient Polymerization Inhibition Systems for Acrylic Acid Distillation: New Liquid-Phase Inhibitors

Identifieur interne : 000581 ( France/Analysis ); précédent : 000580; suivant : 000582

Efficient Polymerization Inhibition Systems for Acrylic Acid Distillation: New Liquid-Phase Inhibitors

Auteurs : Jaroslav Mosnacek [États-Unis, Slovaquie] ; Renaud Nicolay [États-Unis, France] ; Kishore K. Kar [États-Unis] ; Stanley O. Fruchey [États-Unis] ; Michael D. Cloeter [États-Unis] ; Richard S. Harner [États-Unis] ; Krzysztof Matyjaszewski [États-Unis]

Source :

Industrial & engineering chemistry research [ 0888-5885 ] ; 2012.

RBID : Pascal:12-0160652

Descripteurs français

Pascal (Inist)
- Polymérisation, Distillation, Phase liquide.
Wicri :
- topic : Distillation.

English descriptors

KwdEn :
- Distillation, Liquid phase, Polymerization.

Abstract

Phenothiazine and other compounds with similar structures, namely, phenoxazine, promazine, promazine hydrochloride, N,N'-dimethylphenazine, carbazole, N-ethylcarbazole, N-benzylphenothiazine, and N-(1-phenylethyl)phenothiazine were tested as liquid-phase inhibitors for acrylic acid. N-Alkylated phenothiazine (PTZ) derivatives, such as N-benzylphenothiazine and especially N-(1-phenylethyl)phenothiazine, showed improved efficiency for liquid-phase inhibition, in comparison with PTZ. It was also shown that N-alkylated PTZ derivatives could be used in combination with nitroso compounds that can be employed as vapor-phase inhibitors. The combination of N-(1-phenylethyl)phenothiazine and nitrosobenzene showed superior liquid-phase-inhibition efficiency, with time to gelation of >122 h, in comparison with 64 h obtained with PTZ alone. The structure of liquid-phase inhibitors had no influence on the extent of Michael addition reactions during heating of acrylic acid.

Url:

https://hal.archives-ouvertes.fr/hal-00681897

Affiliations:

Links to Exploration step

Pascal:12-0160652

Le document en format XML

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<front><div type="abstract" xml:lang="en">Phenothiazine and other compounds with similar structures, namely, phenoxazine, promazine, promazine hydrochloride, N,N'-dimethylphenazine, carbazole, N-ethylcarbazole, N-benzylphenothiazine, and N-(1-phenylethyl)phenothiazine were tested as liquid-phase inhibitors for acrylic acid. N-Alkylated phenothiazine (PTZ) derivatives, such as N-benzylphenothiazine and especially N-(1-phenylethyl)phenothiazine, showed improved efficiency for liquid-phase inhibition, in comparison with PTZ. It was also shown that N-alkylated PTZ derivatives could be used in combination with nitroso compounds that can be employed as vapor-phase inhibitors. The combination of N-(1-phenylethyl)phenothiazine and nitrosobenzene showed superior liquid-phase-inhibition efficiency, with time to gelation of >122 h, in comparison with 64 h obtained with PTZ alone. The structure of liquid-phase inhibitors had no influence on the extent of Michael addition reactions during heating of acrylic acid.</div>
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Efficient Polymerization Inhibition Systems for Acrylic Acid Distillation: New Liquid-Phase Inhibitors

Efficient Polymerization Inhibition Systems for Acrylic Acid Distillation: New Liquid-Phase Inhibitors

Source :

Descripteurs français

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

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